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1. Choose Window⇒Pixel Dimensions.
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Resistance to 3-hydroxy-3-methylglutaryl coenzyme A reductase inhibitors in a patient with type I hyperlipoproteinemia.
Using a factorial analysis, we examined the basis for primary and secondary resistance to 3-hydroxy-3-methylglutaryl coenzyme A reductase inhibitors (statins) in two patients with type I hyperlipoproteinemia (HLP). Treatment with pravastatin or simvastatin led to normalization of plasma levels of triglycerides and low-density lipoprotein cholesterol, without a concomitant decrease in high-density lipoprotein cholesterol. Lipid profiles of both patients showed only minor changes with other drugs, including bile acid-binding resins, colestipol, gemfibrozil, niacin, and cholestyramine. Plasma concentrations of the statins were stable and plasma drug concentrations determined by HPLC were similar to those reported for patients with type II HLP. Both had the mutant C-292T substitution of the low-density lipoprotein receptor. In contrast, the plasma levels of cholesterol and its components were normal in four other patients with type II HLP who had received similar therapeutic regimens. The two patients also had somatic, rather than germ-line, mutations in the low-density lipoprotein receptor. Their genotypes corresponded to classic heterozygous familial hypercholesterolemia and explained their lipid response to the statins. We conclude that the C-292T mutation of the low-density lipoprotein receptor is associated with primary and secondary resistance to statins in patients with type I HLP.Join Me in My World
Join Me in My World (German: Mit mir in meiner Welt) is a 1936 German comedy film directed by Hans Deppe and starring Wolfgang Zilzer, Hilde Krahl and Valerie Kommissarie.
Wolfgang Zilzer as Walter von Ehrenburg
Hilde Krahl as Ilsa Berlier
Valerie Kommissarie as Ilse – ihre Töchter
Werner Hinz as Erwartungsoffizier
Hans Schumm as Hauptmann von Ehrenberg
Julius Falkenstein as Caféhauswirt
Wolf Hardtenstein as Ferngraf
Oskar Werndorff as Stra
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(1) Field of the Invention
The invention relates to a process for preparing fumaric acid and a catalytic process for catalytically preparing fumaric acid from maleic acid and carbon monoxide and optionally acetic acid.
(2) Background Art
Fumaric acid is used as an acidulant in the preparation of polyethylene terephthalate (PET), which is a condensation product of glycols and terephthalic acid. The terephthalic acid is generally used in the form of dimethyl ester. The dimethyl ester is hydrolyzed to terephthalic acid which is oxidatively polymerized to PET.
Therefore, a continuous production of terephthalic acid is highly desirable. More particularly, direct oxidation of maleic acid by air is an attractive route because of its simplicity and low cost of operation and cost of maleic acid. However, maleic acid is relatively unstable and unless transformed to fumaric acid, spontaneous oxidation of the acid by air during storage would generate oxygenated radicals, and result in undesired polymerization of the acid.
Fumaric acid is a valuable starting material for the preparation of organic compounds. Particularly, it is an important starting material for the production of polyethylene terephthalate.
There is a need for a catalytic process for preparing fumaric acid from maleic acid which does not generate oxygenated radicals.
Fumaric acid can be prepared by carbon monoxide and oxygen or carbon dioxide gas. The patent literature indicates that these reactions can be carried out using a variety of metal catalysts including palladium, rhodium, ruthenium, iridium, platinum and osmium. For example, U.S. Pat. No. 2,968,559 discloses a batch process for preparing fumaric acid using palladium as a catalyst and a carbonaceous reactant such as coal or waste which has been purged of oxygen. U.S. Pat. No. 4,208,458 discloses the preparation of fumaric acid by a batch process using a palladium- or rhodium-containing catalyst.
U.S. Pat. No. 3,803,063 discloses a batch process for preparing fumaric acid from maleic acid using palladium or palladium-containing catalysts supported on silica or alumina. U.S. Pat. No. 3,919,221 discloses the preparation of
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